Articles producció científica> Història i Història de l'Art

Diagnosis of archaeological bones: Analyzing the state of conservation of lower Pleistocene bones through diagenesis methods

  • Identification data

    Identifier: imarina:9379696
    Authors:
    Díaz-Cortés, ADel Valle, HLópez-Polín, LCáceres, IValtierra, NPineda, ASaladié, PVallverdú, JOtero, J
    Abstract:
    Initial physicochemical assessment of cultural materials plays a critical role in the research and management of cultural heritage, serving as a foundation for comprehending deterioration mechanisms and developing effective conservation treatments. However, this knowledge is more advanced in several cultural materials such as artwork or historic buildings, than in bone and fossils. This study focuses on bone material conservation, applying diagenetic methods for characterizing and assessing the state of conservation of archaeological bones from Pit 1 at Barranc de la Boella (BB), an open-air archaeological site from the late Early Pleistocene, from a conservation perspective. Microstructural analyses, including mercury intrusion porosimetry (MIP) and histological analysis, alongside microchemical analyses through Attenuated Total Reflection Fourier Transform Infrared (ATR-FTIR), and FTIR with KBr pellets and X-ray Diffraction (XRD), were conducted to evaluate the decay processes affecting the bones. Results indicated poor bone preservation characterized by high porosity, significant microbial attack, collagen degradation, and the potential recrystallization of bioapatite into fluorapatite. These findings underscore the substantial challenges presented by open-site conditions to preservation efforts and highlight the need for suitable conservation treatments, such as consolidation to reinforce the microstructure. The study emphasizes the importance of characterizing archaeological bones to understand the factors influencing their preservation states and guide conservation works in this material. This work contributes to the knowledge of diagenesis studies to standardize the diagnosis of the state of conservation on archaeological bones.
  • Others:

    Author, as appears in the article.: Díaz-Cortés, A; Del Valle, H; López-Polín, L; Cáceres, I; Valtierra, N; Pineda, A; Saladié, P; Vallverdú, J; Otero, J
    Department: Història i Història de l'Art
    URV's Author/s: Cáceres Cuello de Oro, Isabel / López-Polin Dolhaberriague, Lucía / Saladié Ballesté, Palmira
    Keywords: Archaeological bones Atr Barranc Bioapatit Bioapatite Collagen Conservation diagnosis Consolidant Cultural heritage Delta-o-18 values Diagenesis Fossil Ftir Hydroxyapatite Infrared-spectroscopy Organic-solvent removal Site
    Abstract: Initial physicochemical assessment of cultural materials plays a critical role in the research and management of cultural heritage, serving as a foundation for comprehending deterioration mechanisms and developing effective conservation treatments. However, this knowledge is more advanced in several cultural materials such as artwork or historic buildings, than in bone and fossils. This study focuses on bone material conservation, applying diagenetic methods for characterizing and assessing the state of conservation of archaeological bones from Pit 1 at Barranc de la Boella (BB), an open-air archaeological site from the late Early Pleistocene, from a conservation perspective. Microstructural analyses, including mercury intrusion porosimetry (MIP) and histological analysis, alongside microchemical analyses through Attenuated Total Reflection Fourier Transform Infrared (ATR-FTIR), and FTIR with KBr pellets and X-ray Diffraction (XRD), were conducted to evaluate the decay processes affecting the bones. Results indicated poor bone preservation characterized by high porosity, significant microbial attack, collagen degradation, and the potential recrystallization of bioapatite into fluorapatite. These findings underscore the substantial challenges presented by open-site conditions to preservation efforts and highlight the need for suitable conservation treatments, such as consolidation to reinforce the microstructure. The study emphasizes the importance of characterizing archaeological bones to understand the factors influencing their preservation states and guide conservation works in this material. This work contributes to the knowledge of diagenesis studies to standardize the diagnosis of the state of conservation on archaeological bones.
    Thematic Areas: Administração pública e de empresas, ciências contábeis e turismo Analytical chemistry Astronomia / física Biodiversidade Biotecnología Chemistry, analytical Ciência de alimentos Ciências agrárias i Ciências ambientais Ciências biológicas i Ciências biológicas ii Ciências biológicas iii Enfermagem Engenharias i Engenharias ii Engenharias iii Engenharias iv Farmacia Geociências Interdisciplinar Materiais Medicina i Medicina ii Nutrição Odontología Química Saúde coletiva Spectroscopy
    licence for use: https://creativecommons.org/licenses/by/3.0/es/
    Author's mail: isabel.caceres@urv.cat palmira.saladie@urv.cat lucia.lopezpolin@urv.cat
    Author identifier: 0000-0001-8487-2591 0000-0002-1730-8461 0000-0002-5810-4115
    Record's date: 2024-09-14
    Papper version: info:eu-repo/semantics/publishedVersion
    Papper original source: Microchemical Journal. 206 111353-
    APA: Díaz-Cortés, A; Del Valle, H; López-Polín, L; Cáceres, I; Valtierra, N; Pineda, A; Saladié, P; Vallverdú, J; Otero, J (2024). Diagnosis of archaeological bones: Analyzing the state of conservation of lower Pleistocene bones through diagenesis methods. Microchemical Journal, 206(), 111353-. DOI: 10.1016/j.microc.2024.111353
    Licence document URL: https://repositori.urv.cat/ca/proteccio-de-dades/
    Entity: Universitat Rovira i Virgili
    Journal publication year: 2024
    Publication Type: Journal Publications
  • Keywords:

    Analytical Chemistry,Chemistry, Analytical,Spectroscopy
    Archaeological bones
    Atr
    Barranc
    Bioapatit
    Bioapatite
    Collagen
    Conservation diagnosis
    Consolidant
    Cultural heritage
    Delta-o-18 values
    Diagenesis
    Fossil
    Ftir
    Hydroxyapatite
    Infrared-spectroscopy
    Organic-solvent removal
    Site
    Administração pública e de empresas, ciências contábeis e turismo
    Analytical chemistry
    Astronomia / física
    Biodiversidade
    Biotecnología
    Chemistry, analytical
    Ciência de alimentos
    Ciências agrárias i
    Ciências ambientais
    Ciências biológicas i
    Ciências biológicas ii
    Ciências biológicas iii
    Enfermagem
    Engenharias i
    Engenharias ii
    Engenharias iii
    Engenharias iv
    Farmacia
    Geociências
    Interdisciplinar
    Materiais
    Medicina i
    Medicina ii
    Nutrição
    Odontología
    Química
    Saúde coletiva
    Spectroscopy
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