Articles producció científica> Química Analítica i Química Orgànica

Hypercrosslinked particles for the extraction of sweeteners using dispersive solid-phase extraction from environmental samples

  • Dades identificatives

    Identificador: imarina:5131933
    Autors:
    Lakade SS, Zhou Q, Li A, Borrull F, Fontanals N, Marcé RM.
    Resum:
    This work presents a new extraction material, namely, Q-100, based on hyper-crosslinked magnetic particles, which was tested in dispersive solid-phase extrac-tion for a group of sweeteners from environmental samples. The hypercrosslinkedQ-100 magnetic particles had the advantage of suitable pore size distribution andhigh surface area, and showed good retention behavior toward sweeteners. Di¿erentdispersive solid-phase extraction parameters such as amount of magnetic particles orextraction time were optimized. Under optimum conditions, Q-100 showed suitableapparent recovery, ranging in the case of river water sample from 21 to 88% for allthe sweeteners, except for alitame (12%). The validated method based on dispersivesolid-phase extraction using Q-100 followed by liquid chromatography with tandemmass spectrometry provided good linearity and limits of quanti¿cation between 0.01and 0.1 ¿g/L. The method was applied to analyze samples from river water and e¿u-ent wastewater, and four sweeteners (acesulfame, saccharin, cyclamate, and sucralose)were found in both types of sample.
  • Altres:

    Autor segons l'article: Lakade SS, Zhou Q, Li A, Borrull F, Fontanals N, Marcé RM.
    Departament: Química Analítica i Química Orgànica
    Autor/s de la URV: Borrull Ballarín, Francesc / Fontanals Torroja, Núria / Marcé Recasens, Rosa Maria
    Paraules clau: Sweeteners Liquid chromatography with tandem mass spectrometry Hypercrosslinked magnetic particles Environmental water samples Dispersive solid-phase extraction liquid chromatography with tandem mass spectrometry hypercrosslinked magnetic particles environmental water samples dispersive solid-phase extraction
    Resum: This work presents a new extraction material, namely, Q-100, based on hyper-crosslinked magnetic particles, which was tested in dispersive solid-phase extrac-tion for a group of sweeteners from environmental samples. The hypercrosslinkedQ-100 magnetic particles had the advantage of suitable pore size distribution andhigh surface area, and showed good retention behavior toward sweeteners. Di¿erentdispersive solid-phase extraction parameters such as amount of magnetic particles orextraction time were optimized. Under optimum conditions, Q-100 showed suitableapparent recovery, ranging in the case of river water sample from 21 to 88% for allthe sweeteners, except for alitame (12%). The validated method based on dispersivesolid-phase extraction using Q-100 followed by liquid chromatography with tandemmass spectrometry provided good linearity and limits of quanti¿cation between 0.01and 0.1 ¿g/L. The method was applied to analyze samples from river water and e¿u-ent wastewater, and four sweeteners (acesulfame, saccharin, cyclamate, and sucralose)were found in both types of sample.
    Àrees temàtiques: Química Psicología Medicina ii Medicina i Materiais Linguística e literatura Interdisciplinar Filtration and separation Farmacia Engenharias iii Engenharias ii Engenharias i Ciências da religião e teologia Ciências biológicas ii Ciências biológicas i Ciências ambientais Ciências agrárias i Ciência de alimentos Chemistry, analytical Biotecnología Biodiversidade Analytical chemistry
    Accès a la llicència d'ús: https://creativecommons.org/licenses/by/3.0/es/
    Adreça de correu electrònic de l'autor: nuria.fontanals@urv.cat nuria.fontanals@urv.cat rosamaria.marce@urv.cat francesc.borrull@urv.cat
    Identificador de l'autor: 0000-0002-7534-1964 0000-0002-7534-1964 0000-0002-5667-2899 0000-0003-2718-9336
    Data d'alta del registre: 2024-09-07
    Versió de l'article dipositat: info:eu-repo/semantics/submittedVersion
    Enllaç font original: https://onlinelibrary.wiley.com/doi/abs/10.1002/jssc.201701113
    URL Document de llicència: https://repositori.urv.cat/ca/proteccio-de-dades/
    Referència a l'article segons font original: Journal Of Separation Science. 41 (7): 1618-1624
    Referència de l'ítem segons les normes APA: Lakade SS, Zhou Q, Li A, Borrull F, Fontanals N, Marcé RM. (2018). Hypercrosslinked particles for the extraction of sweeteners using dispersive solid-phase extraction from environmental samples. Journal Of Separation Science, 41(7), 1618-1624. DOI: 10.1002/jssc.201701113
    DOI de l'article: 10.1002/jssc.201701113
    Entitat: Universitat Rovira i Virgili
    Any de publicació de la revista: 2018
    Tipus de publicació: Journal Publications
  • Paraules clau:

    Analytical Chemistry,Chemistry, Analytical,Filtration and Separation
    Sweeteners
    Liquid chromatography with tandem mass spectrometry
    Hypercrosslinked magnetic particles
    Environmental water samples
    Dispersive solid-phase extraction
    liquid chromatography with tandem mass spectrometry
    hypercrosslinked magnetic particles
    environmental water samples
    dispersive solid-phase extraction
    Química
    Psicología
    Medicina ii
    Medicina i
    Materiais
    Linguística e literatura
    Interdisciplinar
    Filtration and separation
    Farmacia
    Engenharias iii
    Engenharias ii
    Engenharias i
    Ciências da religião e teologia
    Ciências biológicas ii
    Ciências biológicas i
    Ciências ambientais
    Ciências agrárias i
    Ciência de alimentos
    Chemistry, analytical
    Biotecnología
    Biodiversidade
    Analytical chemistry
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